NMR USER TRAINING 

	NMR New User Training may be scheduled for 1:00 pm – 2:00 pm on Wednesday, and 1:00 pm – 2:00 pm on Friday. There is a limit of 3 people per session. Contact Claney Pereira (clperei@emory.edu) to make a reservation or for advice. 404-727-6626(lab)
Updated 8/29/2008

Before Attending A Training Session: 

• Print out the Training Request Form, have your advisor sign it, and bring it with you to the training session. (If you are in a rotation, have your current rotations advisor sign the form.)
• Print out the 1H, 13C and Locking & Shimming instructions and bring them with you to the training session. Read them briefly before hand.
• You may bring a sample of your own to the training session. You may practice with your sample TIME PERMITTING. (A typical sample should contain ~5 – 20 mg of sample in 0.7 mL of deuterated solvent.)

Click here to download NMR USER TRAINING REQUEST FORM)

 ¹H instructions file     ¹³C instructions file   Lock and Shim   NMRKEY form

Before you check out:

1. You should practice taking 1H and 13C spectra for several weeks (typically about one month). You should also practice locking and shimming solvents other than CDCl 3.
2. Review the NMR General Handout.

Check out exam: 

For the checkout exam you will be required to take ¹H and ¹³C NMRs, lock a D₂O sample, and accurately shim a shimming standard. You will also be asked to take short (5 question) quiz on commands and safety.

Bring with you an NMR key request form signed by your advisor.

Contact Claney Pereira (clperei@emory.edu) to schedule a checkout exam.

  NMRKEY form

Click here to download NMR USER TRAINING REQUEST FORM

Click here for CHECK-OUT REQUIREMENTS

NMRKEY form

¹H instructions (INOVA400)  ¹³C instructions INOVA400   

¹H instrumction VNMRS400  

¹³C instructions VNMRS400

1D NOE Experiment on VNMRS

COSY Experiment on VNMRS

HMQC/HMBC Experiment on VNMRS

NOESY Experiment on VNMRS

NMR Short Course