1101. Intermittent gain and/or phase problem.

  1. Check to see if the problem happens for one nucleus or for all nuclei.

     

  2. Perform a pw90, ten90, and gain test on the problem nucleus using a short T1 sample.

1102. Image or center peak on the spectrum.

1103. Consistent spikes in spectrum.

  1. Attach a 50-ohm terminator to the probe observe connection, set pw=0, and take an acquisition. If the spikes disappear, the problem is in the transmitter section or probe.

     

  2. Remove the terminator and connect the cable to the probe, leave pw=0, and take an acquisition. If the spikes appear, this may be a probe problem or perhaps the probe is picking up some external signal. If the spikes disappear, the problem is in the transmitter section.

     

  3. If the spikes still appear, the problem is in the receiver section, see faq1017.

1104. Cannot tune probe.

  1. Put the system into probe tune mode and monitor the tune meter with the attenuation switch set to the most sensitive mode.

     

  2. If the meter has no reading, this indicates that there is no output from the transmitter or that the signal is lost within the path to the magnet leg.

     

  3. If the meter has some reading but is not pegged, the output of the transmitter may be low.

     

  4. If the meter is pegged, the transmitter is functional. Follow the probe manual to tune the probe.

     

  5. If the meter has a little reading movement, retune the probe very slowly.

     

  6. If the meter has no movement at all:

    To check transmitter output level, see faq1017.

1105. Noisy baseline (NMR signal is present).

  1. Check using another nuclei and make sure that the observe gain is set to a normal value.

     

  2. Run pw90 test and see if pw90 is flipping normally.

     

  3. If the NMR signal for all of the test nuclei is noisy and pw90 flip is normal, this indicates that the observe preamp and/or observe receiver are defective.

     

  4. If the NMR signal is noisy and the pw90 flip is long, the transmitter is probably defective.

1106. NMR signal or z0 changes daily.

  1. If the signal or z0 is changing downward, this may be the natural drifting of the magnet; however, if the rate of drift is abnormal, you need to monitor the magnet for possible repair.

     

  2. If the signal or z0 changes upward and downward randomly, check the shimming circuitry hardware.

1107. WALTZ birdies when doing WALTZ decoupling.

  1. Verify that the filters are installed inline with the cable to the probe. Use the highpass filter with DEC/Proton channel and the lowpass filter with the OBS/BB channel.

     

  2. Verify that the probe is tuned in both BB and DEC channels.

     

  3. Confirm that the dpwr value is normal by comparing it with the Acceptance Test procedures values.

     

  4. Change the decoupler output to CW mode and verify that the signal is clean.

     

  5. If the above steps are normal, check the probe isolation.

1108. Observing the NMR signal from a second channel

1109. Cannot do deuterium decoupling. (UNITYplus and INOVA only)

  1. Make sure that the cables are connected correctly.

     

  2. Verify that the amplifier is in pulse mode.

     

  3. Compare the lock signal with the lock diplexer installed to the lock signal with no lock diplexer installed.

For a detailed troubleshooting guide, check the chapter on the Lock/Decoupling Accessory in the UNITY Accessory Installation manual.

1110. Spectrum does not decouple with WALTZ (XL,VXR, UNITY only).

  1. Does spectrometer decouple in CW mode?

     

  2. If WALTZ mode cannot be selected, the digital section may be defective. Check or replace the Output board and/or Acquisition Control board.

     

  3. If the WALTZ mode can be selected, check or replace the Master Clock board and/or the Offset Synthesizer board.