NMR SPECTROMETERS:
Updated March 1, 2024
The Emory NMR Research Center houses six Solution NMR spectrometers.
All instruments are located in room 170, Atwood Hall on Emory University main campus. Bruker
AVANCE NEO 800
Commissioned in March 2023, it is equipped with a 5mm triple resonance cryoprobe with
fluorine capability (TCI H&F/C/N-D) and 2H decoupling.
A cooled 24-sloted SampleCase (sample changer) with an Automatic Tuning Module (ATM) on
the probe makes the instrument to run samples automatically. The probe
sensitivity (signal to noise ration): 1H: 8600 13C: 1550 19F: 5500 15N: 80 2H: 12500
It also equipped with a BCU I for variable temperature
experiment. The temperature range is from -40 oC to 85 oC. Bruker
AVANCE III 600
This instrument equipped with a 5 mm BBFO Cryoprobe Prodigy
with Z gradient. The frequency range from 15N-13P, 1H
and 19F.
With ATM (auto-tuning) box installed, the probe is able to
be automatically tuned to observe 1H and 19F on high band
and over a frequency range that enables observation of nuclei between 31P
and 15N on low band. It also has a 24-slot auto sampler which
enables the instrument automatically running day and night. Signal/Noise Ratio: 1H: 1500 13C: 900 19F: 1350 31P: 490 VT temperature range: -40 oC to 85 oC. INOVA
600 The instrument is equipped with an indirect detection
broadband room temperature probe with Z gradient (Variran 600 ID PFG). VT range: 130 oC to -100 oC. There are also a triple
resonance probe and a 3 mm broadband probe for this instrument. VNMRS
400
A 4-nuclei probe is installed. It is capable of running 1H,
19F, 13C and 31P experiments without tuning. Bruker
AVANCE III 400
A BBO (Broadband without 19F) probe is installed
with Z-gradient and an ATM (automatic tuning module). 1H / 31P-15N
are automatically tunable. A 60-slot SampleXpress is installed to enable
automation. Bruker
AVANCE NEO 400
A BBFO (Broadband with 19F) i-probe with
Z-gradient and ATM is installed on this instrument. It can be automatically tuned
from1H/19F to 31P-15N . It is also
equipped a 24-slot SampleCase to run automation using Iconnmr. Signal/Noise Ratio: 1H: 550 13C: 250 19F: 550 31P: 200 |
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