Updated September 1, 2012

The NMR Research Center houses five high resolution Super Conductor-based  NMR spectrometers: Varian   INOVA 600, Bruker AVANCE 600 WB SSNMR, Varian INOVA 400, one Mercury 300 and one VNMRS400) and four workstations  for fast data processing and plotting. Using local network allows researchers to transfer the NMR data to their own laboratory computers.

Multidimensional  studies of such nuclei as 19F, 31P, 183W, 29Si, 51V, 27Al, 2H and 11B are carried out principally with the VNMRS 400 and UNITY Plus 400. The instruments are capable of collecting data for any nucleus of interest at temperatures from -100 oC to 150 oC. The Mercury 300,   INOVA 400 and VNMRS 400 are used principally for chemical structure elucidation. All instruments and computers are available for hands-on use by graduate students, research staff and faculty.

HRMAS, CRAMPS, CPMAS and REDOR and other solid state NMR experiments are available on Bruker Avance 600WB Solid State NMR. 

New users are required, however,  to get necessary training and / or initial authorization in order to use the facility.  

 

 

NMR Spectrometers: 

 INOVA 600

 

14.1T 51mm Bore Oxford Actively shielded Super conducting Magnet. Dual full   band   RF  system  with  PFG  and waveform generators. 1H{X} 5mm PFG Indirect Detection Probe, VT ( - 20C to 80C) ;  1H-19F / 15N-31P 5mm  PFG Switchable  probe ,  VT (- 20C to  60C). 1H {13C/15N}  5mm  PFG  triple probe. Host Sation : SUN SPARC Ultra 5, Data Station: SUN SPARC Ultra 10.

3mm SN60P31P04 BB 009255400 ID 60P54P12 PFG 1H/13C/15N 0099291002

Location: RM211

Installed: November, 1999 (S010861)

 

UNITY Plus 600

(not functional)


It will be replaced by a new 600

 

Location: RM 142

Installed as GE Omega 600 in 1988, Console updated to UNITY in 1999; Console updated to UNITY Plus 2008.

Not functional

 

BRUKER Avance 600WB SOLID

14.1T 89 mm wide bore Bruker Ultrashielded Super conducting Magnet. Three channels. 1H/19F/X (15N - 7Li) 4 mm solid state MAS probe.  1H/X/Y 4mm solid state MAS probe. HRMAS 4mm probe. VT ( -100C to 150C) ; Host Station - SGI O2; Data Station - SGI Octane. Check USER's HALL for basic instructions . 

Installed, November, 2002 Location E125

BH001102

 

INOVA 400

UNITY Plus 400

9.4T 54 mm Bore Oxford  Super Conducting Magnet.  Two  RF   Channels with PFG. 1H/19F/ 13C/31P 5mm 4N/009919200, VT (-20C to 80C); 1H {15N- 31P} 5mm PFG ID probe.

Installed: October, 1996 location: RM211

S009355

9.4T 54 mm Bore Oxford Super Conducting Magnet.  Two  RF  Channels.  5 mm  BB  probe, VT(-100 to 150C); 1H/19F/13C/31P 5mm auto probe, VT (-20C to 80C); 
Installed: May, 1995 Location: VA hospital

 

S008614

 

MERCURY 300 Vx

 

VNMRS 400

7.0T 54mm Bore Oxford  Super Conducting Magnet. 1H/19F/13C/31P 5mm auto switch probe. Host Computer: SUN SPARC Ultra 10

Installed: July, 1998

Location: RM211

S010492 VX

9.4T 54 mm Bore Oxford Super Conducting Magnet.  Two  RF  Channels.  5 mm  BB  probe. Linux OS with VNMRJ2.1B

400SW #0191066100

Installed: April, 2006 Location: RM211

S41142

VNMRS 400     MERCURY 300 Plus  
9.4T 54 mm Bore Varian Conducting Magnet.  Two  RF  Channels.  5 mm  1H/19F/13C/31P  probe. Linux OS with VNMRJ2.1B

Installed: April, 2006

Located RM1093 Rollins

S41176

 

7.0T 54mm Bore Oxford Super Conducting Magnet, ASW probe with VT unitSUN Blade 150 with VNMRJ1.1D Solaris 9.

Installed, October, 2008 (Used, May, 2001)

Location: W W Dept. of Radiology

S010977

 

 

For more detailed information, click here


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