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The NMR Research Center in the Chemistry Department houses eight high
resolution Super Conductor-based NMR spectrometers (INOVA
600, UNITY 600, AVANCE 600 WB SSNMR, INOVA 400, UNITY 400, Mercury 300 and
two VNMRS400) and four
workstations for fast data processing and plotting. Using local network
allows researchers to transfer the NMR data to their own laboratory
computers.
Multidimensional studies of such nuclei as 19F, 31P, 183W, 29Si, 51V, 27Al, 2H and 11B are carried out principally with the VNMRS 400, UNITY 400 and UNITY600. The instruments are capable of collecting data for any nucleus of interest at temperatures from -100 oC to 150 oC. The Mercury 300, INOVA 400 and two new VNMRS are used principally for chemical structure elucidation. All instruments and computers are available for hands-on use by graduate students, research staff and faculty. HRMAS, CRAMPS, CPMAS and REDOR and other solid state NMR experiments are available on Avance 600WB. New users are required, however, to get necessary training and / or initial authorization in order to use the facility. |
NMR Spectrometers:
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INOVA 600 |
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14.1T 51mm Bore Oxford Actively shielded Super conducting Magnet. Dual full band RF system with PFG and waveform generators. 1H{X} 5mm PFG Indirect Detection Probe, VT ( - 20C to 80C) ; 1H-19F / 15N-31P 5mm PFG Switchable probe , VT (- 20C to 60C). 1H {13C/15N} 5mm PFG triple probe. Host Sation : SUN SPARC Ultra 5, Data Station: SUN SPARC Ultra 10. Installed: November, 1999 (S010861) |
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UNITY 600 |
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14.1T 51mm Bore Oxford Actively shielded Super conducting Magnet. Dual full band RF system with PFG and waveform generators. 1H{X} 5mm PFG Indirect Detection Probe, VT ( - 20C to 80C) ; 1H-19F / 15N-31P 5mm PFG Switchable probe , VT (- 20C to 60C). 1H {13C/15N} 5mm PFG triple probe. Host Sation : SUN SPARC Ultra 5, Data Station: SUN SPARC Ultra 10. Installed as GE Omega 600 in 1988, Console updated to UNITY in 1999
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BRUKER 600 SOLID
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14.1T 89 mm wide bore Bruker Ultrashielded Super conducting Magnet. Three channels. 1H/19F/X (15N - 7Li) 4 mm solid state MAS probe. 1H/X/Y 4mm
solid state MAS probe. HRMAS 4mm probe. VT ( -100C to 150C) ; Host Station - SGI O2; Data Station - SGI Octane. Check USER's HALL for basic instructions . Installed, November, 2002 BH001102 |
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INOVA 400 |
UNITY + 400 | |||
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9.4T
54 mm
Bore Oxford
Super Conducting Magnet. Two RF Channels with
PFG. 1H/19F/ 13C/31P 5mm auto probe, VT (-20C to 80C); 1H {15N- 31P} 5mm
PFG ID probe.
Installed: October, 1996(S009355) |
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9.4T
54 mm Bore Oxford Super Conducting Magnet. Two RF
Channels. 5 mm BB probe, VT(-100 to 150C);
1H/19F/13C/31P 5mm auto probe, VT (-20C to 80C); S008614 |
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MERCURY 300 |
VNMRS 400 |
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7.0T
54mm
Bore Oxford Super Conducting Magnet.
1H/19F/13C/31P 5mm auto switch probe. Host Computer: SUN SPARC Ultra 10 Installed: July, 1998 S010492 VX |
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9.4T
54 mm Bore Oxford Super Conducting Magnet. Two RF
Channels. 5 mm BB probe. Linux OS with VNMRJ2.1B Installed: April, 2006 SN41142 |
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9.4T
54 mm Bore Varian Conducting Magnet. Two RF Channels.
5 mm 1H/19F/13C/31P probe. Linux OS with VNMRJ2.1B Installed: April, 2006 Located RM1093 Rollins SN41176 |
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For more detailed information, click here
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