The NMR Research Center in the Chemistry Department houses eight high resolution Super Conductor-based  NMR spectrometers  (INOVA 600, UNITY 600, AVANCE 600 WB SSNMR, INOVA 400, UNITY 400, Mercury 300 and two VNMRS400) and four workstations  for fast data processing and plotting. Using local network allows researchers to transfer the NMR data to their own laboratory computers.

       Multidimensional  studies of such nuclei as 19F, 31P, 183W, 29Si, 51V, 27Al, 2H and 11B are carried out principally with the VNMRS 400, UNITY 400 and  UNITY600. The instruments are capable of collecting data for any nucleus of interest at temperatures from -100 oC to 150 oC. The Mercury 300,   INOVA 400 and two new VNMRS are used principally for chemical structure elucidation. All instruments and computers are available for hands-on use by graduate students, research staff and faculty.

       HRMAS, CRAMPS, CPMAS and REDOR and other solid state NMR experiments are available on Avance 600WB. 

       New users are required, however,  to get necessary training and / or initial authorization in order to use the facility. 
 

 

NMR Spectrometers: 

 INOVA 600

 

        14.1T 51mm Bore Oxford Actively shielded Super conducting Magnet. Dual full   band   RF  system  with  PFG  and waveform generators. 1H{X} 5mm PFG Indirect Detection Probe, VT ( - 20C to 80C) ;  1H-19F / 15N-31P 5mm  PFG Switchable  probe ,  VT (- 20C to  60C). 1H {13C/15N}  5mm  PFG  triple probe. Host Sation : SUN SPARC Ultra 5, Data Station: SUN SPARC Ultra 10.

Installed: November, 1999 (S010861)

 

UNITY 600


 

        14.1T 51mm Bore Oxford Actively shielded Super conducting Magnet. Dual full   band   RF  system  with  PFG  and waveform generators. 1H{X} 5mm PFG Indirect Detection Probe, VT ( - 20C to 80C) ;  1H-19F / 15N-31P 5mm  PFG Switchable  probe ,  VT (- 20C to  60C). 1H {13C/15N}  5mm  PFG  triple probe. Host Sation : SUN SPARC Ultra 5, Data Station: SUN SPARC Ultra 10.

Installed as GE Omega 600 in 1988, Console updated to UNITY in 1999

 

BRUKER 600 SOLID

        14.1T 89 mm wide bore Bruker Ultrashielded Super conducting Magnet. Three channels. 1H/19F/X (15N - 7Li) 4 mm solid state MAS probe.   1H/X/Y 4mm solid state MAS probe. HRMAS 4mm probe. VT ( -100C to 150C) ; Host Station - SGI O2; Data Station - SGI Octane. Check USER's HALL for basic instructions . 

Installed, November, 2002

BH001102

 

INOVA 400

 UNITY + 400

9.4T 54 mm Bore Oxford  Super Conducting Magnet.  Two  RF   Channels with PFG. 1H/19F/ 13C/31P 5mm auto probe, VT (-20C to 80C); 1H {15N- 31P} 5mm PFG ID probe.

Installed: October, 1996(S009355)

9.4T 54 mm Bore Oxford Super Conducting Magnet.  Two  RF  Channels.  5 mm  BB  probe, VT(-100 to 150C); 1H/19F/13C/31P 5mm auto probe, VT (-20C to 80C); 
Installed: May, 1995

S008614
 

MERCURY 300

  

VNMRS 400

7.0T 54mm Bore Oxford  Super Conducting Magnet. 1H/19F/13C/31P 5mm auto switch probe. Host Computer: SUN SPARC Ultra 10

Installed: July, 1998

S010492 VX

9.4T 54 mm Bore Oxford Super Conducting Magnet.  Two  RF  Channels.  5 mm  BB  probe. Linux OS with VNMRJ2.1B

Installed: April, 2006

SN41142
         
9.4T 54 mm Bore Varian Conducting Magnet.  Two  RF  Channels.  5 mm  1H/19F/13C/31P  probe. Linux OS with VNMRJ2.1B

Installed: April, 2006

Located RM1093 Rollins

SN41176

     

 

 

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